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This test method covers the use of both pyridine and pyridine-free KF reagents for determining water by the volumetric titration. Determination of water using KF coulometric .Our portfolio of Karl Fischer titrators includes compact all-in-one options for routine moisture determination as well as fully automated Karl Fischer systems for volumetric and . Scope1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or liquid organic and inorganic compounds. This test method is desig . ASTM grants Licensee a limited, revocable, nonexclusive, non-transferable license to .

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1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or liquid organic and inorganic compounds. This test method is designed for use with automatic titration systems capable of determining the KF titration end point potentiometrically; however, a .E203 Test Method for Water Using Volumetric Karl Fischer Titration E1064 Test Method for Water in Organic Liquids by Coulo-metric Karl Fischer Titration 3. Terminology 3.1 For general terminology, refer to Terminology D4175. 4. Summary of Test Method 4.1 This method uses Karl Fischer titration to determine the amount of water in a sample.1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or liquid organic and inorganic compounds. This test method is designed for use with automatic titration systems capable of determining the KF titration end point potentiometrically; however, a .Karl Fischer Moisture Titrator: Model: MKV-710D: Standard configuration: MCU-710D+MKV-710+Automatic Solvent Change unit: Measuring method: Karl Fischer Volumetric titration: Measuring range: 1) Water content : 0.1 to 500mgH 2 O (depends on KF reagent factor) 2) Concentration : 1ppm to 100%H 2 O: Burette precision: 10mL burette +/- 0.015mL .

Titration techniques using KF reagent are one of the most widely used for the determination of water. Although the volumetric KF titration can determine low levels of water, it is generally accepted that coulometric KF titrations (see Test Method E 1064) are more accurate for routine determination of very low levels of water.As a general rule, if samples routinely .

4.1 The coulometric technique is especially suited for determining low concentrations of water in organic liquids that would yield small titers by the Karl Fischer volumetric procedure. The precision and accuracy of the coulometric technique decreases for concentrations of water much greater than 2.0 % because of the difficulty in measuring the . Water in Solids by Furnace Desorption with Volumetric Karl Fischer Titration UOP993-15 UOP . ASTM grants Licensee a limited, revocable, nonexclusive, non-transferable license to access, by means of one or more authorized IP addresses, and according to the terms of this Agreement, to make the uses permitted and described below, each ASTM . USA Testing Lab for ASTM E203 Water Content Analysis Using Volumetric Karl Fischer Titration in USA, Indonesia, Philippines, Malaysia, Thailand, Canada, China, India, and all over the World. (302)244-7710 . [email protected] . FREE Consultation Services . Materials testing .

Standard Test Method for Water in Lint Cotton by Oven Evaporation Combined with Volumetric Karl Fischer Titration D7785-12 ASTM|D7785-12 . ASTM grants Licensee a limited, revocable, nonexclusive, non-transferable license to access, by means of one or more authorized IP addresses, and according to the terms of this Agreement, to make the uses .Karl Fischer Moisture Titrator: Model: MKV-710S: Standard configuration: MCU-710S+MKV-710+IDP-100+Manual Solvent Change unit: Measuring method: Karl Fischer Volumetric titration: Measuring range: 1) Water content : 0.1 to 500mgH 2 O (depends on KF reagent factor) 2) Concentration : 1ppm to 100%H 2 O: Burette precision: 10mL burette +/- 0.015mL .Karl Fischer Moisture Titrator: Model: MKV-710B: Standard configuration: MKV-710+IDP-100+Manual Solvent Change unit: Measuring method: Karl Fischer Volumetric titration: Measuring range: 1) Water content : 0.1 to 500mgH 2 O (depends on KF reagent factor) 2) Concentration : 1ppm to 100%H 2 O: Burette precision: 10mL burette +/- 0.015mL . Water Using Volumetric Karl Fischer Titration 1 This standard is issued under the ®xed designation E203; the number immediately following the designation indicates the year of . 2.1 A list of existing ASTM Karl Fischer methods, their applications to various products, and the sponsoring commit-tees is given in Appendix X3. 2.2 ASTM Standards: 2

Standard Practice for Water in Lint Cotton by Oven Evaporation Combined with Volumetric Karl Fischer Titration D7785-21 ASTM|D7785-21 . ASTM grants Licensee a limited, revocable, nonexclusive, non-transferable license to access, by means of one or more authorized IP addresses, and according to the terms of this Agreement, to make the uses .

2.1 ASTM Standards:2 D1193 Speciﬁcation for Reagent Water . E203 Test Method for Water Using Volumetric Karl Fischer Titration 2.2 API Standards:3 MPMS Chapter 8.1 Manual Sampling of Petroleum and Petroleum Products (ASTM Practice D4057) MPMS Chapter 8.2 Automatic Sampling of Petroleum and Petroleum Products (ASTM Practice D4177)ASTM E203-01 Standard Test Method for Water Using Volumetric Karl Fischer Titration. 1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and . Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration D4928-12R18 ASTM|D4928-12R18 . Internet traffic volume, upgrades, overload of requests to servers, general network failures or delays, or any other cause that may from time to time make the Product unavailable for the Licensee or Licensee's Authorized Users. .

Automated titration is an accessory offered by some Karl Fischer manufacturers that allows the user to perform multiple titrations without stopping to prepare a sample. It is combined with either a coulometric or volumetric Karl Fischer titrator to determine the amount of water in the sample efficiently and unmonitored, allowing the analyst to .

There are two types of Karl Fischer titration: volumetric and coulometric titrations. [3] Volumetric titration relies on carefully measuring the volume of a Karl Fischer reagent – a solution containing iodine, sulfur dioxide, a base, and a solvent – that reacts with water in the sample. The reaction between the Karl Fischer reagent and . 6 Karl Fischer Titration | July 2018 | Merck KGaA | Bettina Straub-Jubb Karl Fischer Titration Method for Water Determination Karl Fischer method is one of the most used methods for water determination while: Selective for water Universally applicable (10 ppm –100%) Fast method (short titration time, few minutes) Accurate and precise

Karl Fischer Moisture Titrator: Model: MKV-710M: Standard configuration: MCU-710M+MKV-710+IDP-100+Manual Solvent Change unit: Measuring method: Karl Fischer Volumetric titration: Measuring range: 1) Water content : 0.1 to 500mgH 2 O (depends on KF reagent factor) 2) Concentration : 1ppm to 100%H 2 O: Burette precision: 10mL burette +/- 0.015mL .Water Using Volumetric Karl Fischer Titration 1 . 2.1 A list of existing ASTM Karl Fischer methods, their applications to various products, and the sponsoring commit-tees is given in Appendix X3 . 2.2 ASTM Standards: 2 D 789 Test Methods for Determination of Solution Viscosi-This Karl Fischer Titration Guide Part 1 explains the chemical reaction and the two major measuring techniques: volumetry and coulometry. It also presents a short, historic overview of the development of Karl Fischer’s method. . Volumetric Karl Fischer Titration, where a solution containing iodine is added using a motorized piston burette;ASTM E203-08 Standard Test Method for Water Using Volumetric Karl Fischer Titration. 1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or liquid organic and inorganic compounds. This test method is designed for use .

Karl Fischer, moisture, titration, water 1 | INTRODUCTION The measurement of water in a material is crucial to determine the consistency of the product, and shelf life, or as a characterization technique.[1] Various methods, including loss on drying tests, electronic methods, near-infrared spectroscopy, and Karl Fischer (KF) titrators, based on ASTM E203, Standard Test Method for Water Using Volumetric Karl Fischer Titration [3]. This standard test method is specified for measuring the mass % water in pyrolysis liquid biofuels in ASTM D7544, Standard Specification for Pyrolysis Liquid Biofuel [4]. Although the standard method is prescribed for the analysis of pyrolysisScope 1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or liquid organic and inorganic compounds. This test method is designed for use with automatic titration systems capable of determining the KF titration end .

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